HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiomorpholine → HCID 57496144, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiomorpholine | HCID 67164 | — |
| Reactant | 4-(3-(3-cyanophenyl)ureido)-N-(4-sulfamoylbenzyl)benzenesulfonamide | HCID 57496180 | — |
| Product | HCID 57496144 | HCID 57496144 | 28% |
Reaction Steps
The title compound was prepared from 4-(3-(3-cyanophenyl)ureido)-N-(4-sulfamoylbenzyl)benzenesulfonamide following procedure C and using 1.1 equivalents of thiomorpholine as secondary amine. The product was purified by preparative TLC (eluent DCM/MeOH 8:2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08343963B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-37ff793aa8414b0db1fc2ee20fb92a6f |
| Source note | uspto-grants-2013_01 |