HCID 58292666, compound → HCID 58292740, compound

Participants

Reaction Steps

To a solution of ethyl 2-(1-hydroxy-4-methyl-6-(2-nitropyridin-4-yloxy)-1,3-dihydrobenzo[c][1,2]oxaborol-3-yl)acetate in 2M ammonia in ethanol was added 1 ml Raney-Nickel (slurry in water). The mixture was stirred at room temperature for 8 hours and then filtered through Celite. The filtrate was evaporated to yield desired product. MS (ESI) m/z=343 [M+H]+.

Provenance & Evidence