HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Fluoro-3,5-dimethoxyphenyl)furan → HCID 58432107, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Fluoro-3,5-dimethoxyphenyl)furan | HCID 58431998 | — |
| Reactant | N,2-dimethoxy-N-methyl-2-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl)acetamide | HCID 58432086 | — |
| Product | HCID 58432107 | HCID 58432107 | — |
Reaction Steps
1-(5-(4-Fluoro-3,5-dimethoxyphenyl)furan-2-yl)-2-methoxy-2-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl)ethanone was prepared from 2-(4-fluoro-3,5-dimethoxyphenyl)furan and N,2-dimethoxy-N-methyl-2-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl)acetamide according to the procedure used in Example 30. Purification by chromatography (60% EtOAc-hexanes) gave the product as a pale yellow solid (0.036 g, 8% yield). MS: m/z 453.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08343970B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-e88b84f40cf54cf69ebd51bd1cf70177 |
| Source note | uspto-grants-2013_01 |