HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl (2E)-3-{3-fluoro-2-[(triphenylphosphoranylidene)amino]phenyl}propenoate → HCID 58941058, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl (2E)-3-{3-fluoro-2-[(triphenylphosphoranylidene)amino]phenyl}propenoate | HCID 11983908 | — |
| Reactant | Benzene, 2-isocyanato-1-methoxy-4-(trifluoromethyl)- | HCID 11983909 | — |
| Reactant | 8-Fluoro-1,2,3,4-tetrahydropyrazino[1,2-a]indole | HCID 45115769 | — |
| Product | HCID 58941058 | HCID 58941058 | — |
Reaction Steps
Starting with 182 mg (0.4 mmol) of the irninophosphorane from Example 12A, 86 mg of 2-isocyanato-1-methoxy-4-(trifluoromethyl)benzene and 130 mg (0.4 mmol) of 8-fluoro-1,2,3,4-tetrahydropyrazino[1,2-a]indole from Example 36A, the general procedure [M] gives 95 mg (35% of theory) of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08343981B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-0268c5bd11d14553a81591f3d69dc007 |
| Source note | uspto-grants-2013_01 |