Clopyralid → HCID 178431967, compound

Participants

Reaction Steps

Compound of Production Example 3 can be produced by the same method as Production Example 1, by a method according thereto, or by a combination of these and ordinary methods with the use of 3,6-dichloro-2-pyridinecarboxylic acid, 2-amino-4-methylthiazole, 4-fluoro-thiophenol and 3-mercapto-1,2,4-triazole. 1HNMR (CDCl3) δ: 2.40 (3H, s), 6.61 (1H, s), 7.01 (1H, d, J=9.3 Hz), 7.17-7.25 (3H, m), 7.58 (2H, m), 8.35 (1H, s) ESI-MS (m/e): 445 [M+H]+

Provenance & Evidence