HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68663612, compound → HCID 68665323, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68663612 | HCID 68663612 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68665323 | HCID 68665323 | — |
Reaction Steps
PCC (13.61 g, 63.28 mmol) was added to a solution of compound F (20 g, 42.19 mmol) in DCM (400 mL). The mixture was stirred at RT overnight and filtered through a pad of celite. The filtrate was concentrated and purified by column chromatography to obtain 8.5 g (33%, two steps) of compound G.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08343996B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-b6f1ac91e887418d9b10fab9143c33f5 |
| Source note | uspto-grants-2013_01 |