反应详情

PCC (21.19 g, 98.58 mmol) was added to a solution of compound F (28 g, 65.72 mmol) in DCM (550 mL). The mixture was stirred at RT overnight and filtered through a pad of celite. The filtrate was concentrated and purified by column chromatography to obtain 16 g (46%, 2 steps) of compound G.

1. filtrationfiltered through a pad of celite
2. concentrationThe filtrate was concentrated
3. custompurified by column chromatography