HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylparaben → N-{4-[2-(4-Methoxyphenyl)ethoxy]benzoyl}glycine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylparaben | HCID 7456 | — |
| Reactant | 4-Methoxyphenethyl alcohol | HCID 69705 | — |
| Reactant | N-[4-(2-Cyclopropylethoxy)benzoyl]glycine | HCID 66812105 | — |
| Product | N-{4-[2-(4-Methoxyphenyl)ethoxy]benzoyl}glycine | HCID 66812093 | 79% |
Reaction Steps
Reactions similar to those described in Example 1 (1a) and (1b) were conducted using methyl 4-hydroxybenzoate (4.56 g, 30.0 mmol) and 2-(4-methoxyphenyl)ethanol (5.03 g, 33.0 mmol) to give 7.80 g of the title compound (white powder, yield: 79%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08344029B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-5190dba4f85c4f16bff6c6b983662061 |
| Source note | uspto-grants-2013_01 |