HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylparaben → N-[4-(Cyclopentylmethoxy)benzoyl]glycine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylparaben | HCID 7456 | — |
| Reactant | Cyclopentanemethanol | HCID 77195 | — |
| Reactant | N-[4-(2-Cyclopropylethoxy)benzoyl]glycine | HCID 66812105 | — |
| Product | N-[4-(Cyclopentylmethoxy)benzoyl]glycine | HCID 69017052 | 35% |
Reaction Steps
Reactions similar to those described in Example 1 (1a) and (1b) were conducted using methyl 4-hydroxybenzoate (22.8 g, 150 mmol) and cyclopentylmethanol (10.0 g, 100 mmol) to give 9.3 g of the title compound (colorless crystal, yield: 35%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08344029B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-6a4614211d8345e7bb0d7db9da2878be |
| Source note | uspto-grants-2013_01 |