1-Heptanol, 7-bromo- → HCID 66875085, compound
Reaction equation
[C:1]1([CH2:7][CH2:8][SH:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Br[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][OH:18]>>[CH2:8]([S:9][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][OH:18])[CH2:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1Participants
3
Procedure
2-Phenylethanethiol was alkylated with 7-bromo-1-heptanol in analogy with example 18, step 1, affording 7-phenethylsulfanyl-heptan-1-ol.
Sources & evidence
- ORD record
- ord-775165271d7644b3acb5dd4d9a91d449
- Source dataset
- uspto-grants-2013_01
- Patent number
- US08344027B2
Reaction notes
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