Ethanol → HCID 86609815, compound

HRID 1799693Notes

Reaction equation

HRID 1799693 reaction equation
[CH2:1]([O:3][C:4]([C:6]1[N:7]=[C:8](I)[S:9][C:10]=1[C:11]([O:13][CH2:14][CH3:15])=[O:12])=[O:5])[CH3:2].[CH2:17](O)[CH3:18]>CO>[CH2:1]([O:3][C:4]([C:6]1[N:7]=[C:8]([C:17]#[CH:18])[S:9][C:10]=1[C:11]([O:13][CH2:14][CH3:15])=[O:12])=[O:5])[CH3:2]

Participants

4

Reactant 2

HCID 702EthanolHCID 68600380HCID 68600380, compound

Product 1

HCID 86609815HCID 86609815, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

4,5-Diethoxycarbonyl-2-ethynylthiazole (539 mg) was prepared from 1.16 g of 4,5-diethoxycarbonyl-2-iodothiazole in the same manner as in step b) in Example 4, except that ethanol was used as the solvent instead of methanol.

Sources & evidence

ORD record
ord-053971c946be4f879ec00bb7b50f261e
Source dataset
uspto-grants-2013_01
Patent number
US08344154B2

Reaction notes

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