HRID1799899

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID78740

1-(2,2,2-Trifluoroethyl)hydrazine

C2H5F3N2

结构：CN(C)C=NC(=O)c1cc2n(n1)-c1cc(Br)ccc1OCC2

HCID58204417

未命名化合物

结构：CC(C)n1ncnc1-c1cc2n(n1)-c1cc(Br)ccc1OCC2

HCID58204730

未命名化合物

PRODUCTS

生成物

结构：FC(F)(F)Cn1ncnc1-c1cc2n(n1)-c1cc(Br)ccc1OCC2

HCID58204989

未命名化合物

PROCEDURE

实验过程

Following the procedure for 9-bromo-2-(2-isopropyl-2H-[1,2,4]triazol-3-yl)-4,5-dihydro-6-oxa-1,10b-diaza-benzo[e]azulene, 9-bromo-4,5-dihydro-6-oxa-1,10b-diaza-benzo[e]azulene-2-carboxylic acid 1-dimethylaminomethylideneamide was reacted with trifluoroethyl hydrazine (70% aqueous) to give 9-Bromo-2-[2-(2,2,2-trifluoro-ethyl)-2H-[1,2,4]triazol-3-yl]-4,5-dihydro-6-oxa-1,10b-diaza-benzo[e]azulene as a white solid. LCMS RT=4.49 min, M+H+=414/416.