HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluoro-4-(2-(4-methylpyridin-2-ylamino)thiazol-5-ylthio)picolinic acid → HCID 59321366, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluoro-4-(2-(4-methylpyridin-2-ylamino)thiazol-5-ylthio)picolinic acid | HCID 59200397 | — |
| Reactant | HCID 59321431 | HCID 59321431 | — |
| Product | HCID 59321366 | HCID 59321366 | — |
Reaction Steps
Following the amide bond forming procedure given in example 37, 3-fluoro-4-(2-(4-methylpyridin-2-ylamino)thiazol-5-ylthio)picolinic acid (intermediate B in example 1) and tert-butyl 4-(aminomethyl)-4-(3,4-dichlorophenyl)piperidine-1-carboxylate (amine intermediate “K”) were reacted to give the title compound. LC/MS (M+H)+: 703. Ret. time: 2.20 min. (Condition I).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08343999B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-e7f944124fef43aa982067f4259c2ec6 |
| Source note | uspto-grants-2013_01 |