HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → HCID 59321412, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | HCID 59321379 | HCID 59321379 | — |
| Product | HCID 59321412 | HCID 59321412 | — |
Reaction Steps
Following the procedure given for example 81, N-((4-(3,4-dichlorophenyl)piperidin-4-yl)methyl)-3-fluoro-4-(2-(4-methylpyridin-2-ylamino)thiazol-5-ylthio)picolinamide (compound example 48) was reacted with methyl chloroformate to give the title compound. LC/MS (M+H)+: 661. Ret. time: 2.09 min. (Condition I); analytical HPLC Ret. time: 10.35 min (Condition H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08343999B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-379cff98930f4f97a233a26f1903bc60 |
| Source note | uspto-grants-2013_01 |