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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1801325Generated: November 2, 2026

Methyl 4-aminobenzoate → HCID 178498133, compound

https://huagongshe.com/reaction/1801325

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl 4-aminobenzoateHCID 12082—
Reactant3-Chloro-5-nitrobenzaldehydeHCID 12248973—
SolventEthanolHCID 702—
ProductHCID 178498133HCID 1784981331,085.6%

Reaction Steps

To a solution of 3-chloro-5-nitrobenzaldehyde (371 mg, 0.1 mmol) in ethanol (6 mL) was added methyl 4-aminobenzoate (302 mg, 2.0 mmol). After a while, solids precipitated from the resulting clear yellow solution. The precipitated solid was filtered and 346 mg of (E)-methyl 4-(3-chloro-5-nitrobenzylideneamino)benzoate as a yellow solid was obtained. Yield=54%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08344137B2
Source datasetuspto-grants-2013_01
ORD IDord-0f8aff8f88e04e9e80e358b7dd3184dc
Source noteuspto-grants-2013_01