HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-aminobenzoate → HCID 178498133, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-aminobenzoate | HCID 12082 | — |
| Reactant | 3-Chloro-5-nitrobenzaldehyde | HCID 12248973 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178498133 | HCID 178498133 | 1,085.6% |
Reaction Steps
To a solution of 3-chloro-5-nitrobenzaldehyde (371 mg, 0.1 mmol) in ethanol (6 mL) was added methyl 4-aminobenzoate (302 mg, 2.0 mmol). After a while, solids precipitated from the resulting clear yellow solution. The precipitated solid was filtered and 346 mg of (E)-methyl 4-(3-chloro-5-nitrobenzylideneamino)benzoate as a yellow solid was obtained. Yield=54%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08344137B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-0f8aff8f88e04e9e80e358b7dd3184dc |
| Source note | uspto-grants-2013_01 |