HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaric Acid → HCID 66885603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | HCID 11978936 | HCID 11978936 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66885603 | HCID 66885603 | — |
Reaction Steps
Fumaric acid was added to an ethanol solution of 7-[3-(4-benzo[b]thiophen-4-yl-piperazin-1-yl)propoxy]-2-methyl-3,4-dihydro-2H-isoquinolin-1-one and the solvent was evaporated under reduced pressure. The residue was recrystallized from 70% ethanol and thereby 7-[3-(4-benzo[b]thiophen-4-yl-piperazin-1-yl)propoxy]-2-methyl-3,4-dihydro-2H-isoquinolin-1-one fumarate was obtained in the form of a pale yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08349840B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-b748945c247d412aa62b5626e81b258a |
| Source note | uspto-grants-2013_01 |