HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carzenide → HCID 16068462, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carzenide | HCID 8739 | — |
| Reactant | HCID 178513405 | HCID 178513405 | — |
| Product | HCID 16068462 | HCID 16068462 | — |
Reaction Steps
The title compound was prepared from N-hydroxy-4-trifluoromethyl-2-(4-trifluoromethyl-phenyl)-imidazo[1,5-a]pyrimidine-8-carboxamidine (example B.3) (195 mg, 0.5 mmol) and commercially available 4-sulfamoyl-benzoic acid (101 mg, 0.5 mmol) according to general procedure II. Obtained after purification by column chromatography (dichloromethane/MeOH/NH4OH) and crystallization (dichloromethane) as a yellow solid (61 mg, 22%). MS (ISP) 555.3 [(M+H)+]; mp 303° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08349844B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-e3a6236b47a4415f9cd3f49bd54121b1 |
| Source note | uspto-grants-2013_01 |