N-Methylethylamine → HCID 58446871, compound

HRID 1802272Notes

Reaction equation

HRID 1802272 reaction equation
[CH3:1][N:2]1[CH:6]=[C:5]([C:7]([OH:9])=O)[CH:4]=[N:3]1.[CH3:10][NH:11][CH2:12][CH3:13]>>[CH2:12]([N:11]([CH3:10])[C:7]([C:5]1[CH:4]=[N:3][N:2]([CH3:1])[CH:6]=1)=[O:9])[CH3:13]

Participants

3

Reactant 2

HCID 12219N-MethylethylamineHCID 6431601-Methyl-1H-pyrazole-4-carboxylic acid

Product 1

HCID 58446871HCID 58446871, compound

Procedure

This compound was prepared in the same manner as described in example 97, step a from 1-methyl-1H-pyrazole-4-carboxylic acid (1.0 g, 7.93 mmol) and N-methylethanamine (715 μl, 8.33 mmol). Yield: 995 mg (75%); off-white solid; MS: m/z=168.1 [M+H]+.

Workup

  1. customThis compound was prepared in the same manner

Sources & evidence

ORD record
ord-71632d6609fc48e4a1df97e5bc4fd392
Source dataset
uspto-grants-2013_01
Patent number
US08349824B2

Reaction notes

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