(2-Methoxyethyl)(methyl)amine → HCID 58446939, compound

HRID 1802273Notes

Reaction equation

HRID 1802273 reaction equation
[CH3:1][N:2]1[CH:6]=[C:5]([C:7]([OH:9])=O)[CH:4]=[N:3]1.[CH3:10][O:11][CH2:12][CH2:13][NH:14][CH3:15]>>[CH3:10][O:11][CH2:12][CH2:13][N:14]([CH3:15])[C:7]([C:5]1[CH:4]=[N:3][N:2]([CH3:1])[CH:6]=1)=[O:9]

Participants

3

Reactant 2

HCID 300977(2-Methoxyethyl)(methyl)amineHCID 6431601-Methyl-1H-pyrazole-4-carboxylic acid

Product 1

HCID 58446939HCID 58446939, compound

Procedure

This compound was prepared in the same manner as described in example 97, step a starting from 1-methyl-1H-pyrazole-4-carboxylic acid (500 mg, 3.96 mmol) and 2-methoxy-N-methylethanamine (389 mg, 4.36 mmol). Yield: 580 mg (74%); colorless liquid; MS: m/z=198.1 [M+H]+.

Workup

  1. customThis compound was prepared in the same manner

Sources & evidence

ORD record
ord-9981565ee73f47e89acd68d5928b653d
Source dataset
uspto-grants-2013_01
Patent number
US08349824B2

Reaction notes

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