HCID 59436021, compound → HCID 178467404, compound

HRID 1802486Notes

Reaction equation

HRID 1802486 reaction equation
N[C:2]1[CH:7]=[CH:6][N:5]=[CH:4][C:3]=1[C:8]1[C:9]([O:23][CH2:24][CH3:25])=[N:10][CH:11]=[CH:12][C:13]=1[C:14]([N:16](C(C)C)C(C)C)=[O:15].NC1C=CN=CC=1C1C(OCC)=CC=CC=1C(OC)=O>>[CH2:24]([O:23][C:9]1[C:8]2[C:3]3[C:2](=[CH:7][CH:6]=[N:5][CH:4]=3)[N:16]=[C:14]([OH:15])[C:13]=2[CH:12]=[CH:11][N:10]=1)[CH3:25]

Participants

3

Reactant 2

HCID 59436021HCID 59436021, compoundHCID 68421079HCID 68421079, compound

Product 1

HCID 178467404HCID 178467404, compound

Procedure

4′-Amino-2-ethoxy-N,N-diisopropyl-3,3′-bipyridine-4-carboxamide was converted to methyl 2-(4-aminopyridin-3-yl)-3-ethoxybenzoate using the same procedure as shown in (Example 3, Step 2). The product was triturated with diethyl ether.

Workup

  1. customThe product was triturated with diethyl ether

Sources & evidence

ORD record
ord-fb57b72e48a34fd7a981918a570a7d9a
Source dataset
uspto-grants-2013_01
Patent number
US08349865B2

Reaction notes

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