2-Acetylpyridine → HCID 68476582, compound

HRID 1802800Notes

Reaction equation

HRID 1802800 reaction equation
Cl.[CH3:2][C:3]1[CH:8]=[CH:7][C:6]([NH:9]N)=[C:5]([N+:11]([O-:13])=[O:12])[CH:4]=1.[C:14]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][N:18]=1)(=O)[CH3:15]>>[CH3:2][C:3]1[CH:8]=[C:7]2[C:6](=[C:5]([N+:11]([O-:13])=[O:12])[CH:4]=1)[NH:9][C:14]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][N:18]=1)=[CH:15]2

Participants

3

Reactant 2

HCID 142862-AcetylpyridineHCID 16495251HCID 16495251, compound

Product 1

HCID 68476582HCID 68476582, compoundYield 16.1%

Procedure

(4-Methyl-2-nitrophenyl)hydrazine hydrochloride (10 g, 49 mmol) and 2-acetylpyridine (5.5 ml, 49 mmol) were reacted according to the same procedures as Preparations 4 to 5 to give the title compound (2 g, Yield 16%).

Sources & evidence

ORD record
ord-43fba216fefd4f2a910ed8e53ac5e88a
Source dataset
uspto-grants-2013_01
Patent number
US08349885B2

Reaction notes

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