2-Acetylpyridine → HCID 59576157, compound

HRID 1802804Notes

Reaction equation

HRID 1802804 reaction equation
Cl.[CH2:2]([O:4][C:5]1[CH:10]=[CH:9][C:8]([NH:11]N)=[C:7]([N+:13]([O-:15])=[O:14])[CH:6]=1)[CH3:3].[C:16]([C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][N:20]=1)(=O)[CH3:17]>>[CH2:2]([O:4][C:5]1[CH:10]=[C:9]2[C:8](=[C:7]([N+:13]([O-:15])=[O:14])[CH:6]=1)[NH:11][C:16]([C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][N:20]=1)=[CH:17]2)[CH3:3]

Participants

3

Reactant 2

HCID 142862-AcetylpyridineHCID 68635538HCID 68635538, compound

Product 1

HCID 59576157HCID 59576157, compoundYield 8.4%

Procedure

(4-Ethoxy-2-nitrophenyl)hydrazine hydrochloride (5 g, 21 mmol) and 2-acetylpyridine (2.4 ml, 21 mmol) were reacted according to the same procedures as Preparations 4 to 5 to give the title compound (0.5 g, Yield 8%).

Sources & evidence

ORD record
ord-2feeacfd759b426f87693b85df9fbf5f
Source dataset
uspto-grants-2013_01
Patent number
US08349885B2

Reaction notes

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