HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethynylcyclohexane → 2-cyclohexyl-5-methyl-7-nitro-1H-indole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethynylcyclohexane | HCID 70263 | — |
| Edukt | 2-Iodo-4-methyl-6-nitroaniline | HCID 19735199 | — |
| Produkt | 2-cyclohexyl-5-methyl-7-nitro-1H-indole | HCID 68634331 | 62,4% |
Reaktionsschritte
6-Iodo-4-methyl-2-nitroaniline (500 mg, 1.8 mmol) and cyclohexylacetylene (0.23 ml, 1.8 mmol) were reacted according to the same procedure as Preparation 19 to give the title compound (290 mg, Yield 62%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08349885B2 |
| Quelldatensatz | uspto-grants-2013_01 |
| ORD ID | ord-757b1467e67e408fb9f30e363d61e28a |
| Quellennotiz | uspto-grants-2013_01 |