Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Ethynyl-6-methylpyridine → 5-Methyl-2-(6-methyl-pyridin-2-yl)-7-nitro-1h-indole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Ethynyl-6-methylpyridine | HCID 13400635 | — |
| 반응물 | 2-Iodo-4-methyl-6-nitroaniline | HCID 19735199 | — |
| 생성물 | 5-Methyl-2-(6-methyl-pyridin-2-yl)-7-nitro-1h-indole | HCID 68634447 | 35.3% |
반응 단계
6-Iodo-4-methyl-2-nitroaniline (500 mg, 1.8 mmol) and 2-ethinyl-6-methylpyridine (210 mg, 1.8 mmol) were reacted according to the same procedure as Preparation 19 to give the title compound (170 mg, Yield 35%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08349885B2 |
| 출처 데이터셋 | uspto-grants-2013_01 |
| ORD ID | ord-e7e78dc0cebe47cfa957790382653b10 |
| 출처 메모 | uspto-grants-2013_01 |