HCID 67241477, compound → HCID 67239262, compound

HRID 1802864Notes

Reaction equation

HRID 1802864 reaction equation
C([O:8][C:9]1[CH:14]=[CH:13][C:12]([F:15])=[CH:11][C:10]=1[C:16]1[CH:21]=[CH:20][C:19]([S:22]([C:25]2[CH:30]=[CH:29][C:28]([O:31][CH3:32])=[CH:27][CH:26]=2)(=[O:24])=[O:23])=[C:18]([F:33])[CH:17]=1)C1C=CC=CC=1>C(O)(=O)C.[Pd]>[F:33][C:18]1[CH:17]=[C:16]([C:10]2[C:9]([OH:8])=[CH:14][CH:13]=[C:12]([F:15])[CH:11]=2)[CH:21]=[CH:20][C:19]=1[S:22]([C:25]1[CH:26]=[CH:27][C:28]([O:31][CH3:32])=[CH:29][CH:30]=1)(=[O:23])=[O:24]

Participants

4

Reactant 1

HCID 67241477HCID 67241477, compound

Product 1

HCID 67239262HCID 67239262, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 176Acetic AcidSolvent

Procedure

The subtitle compound was prepared by the method of example 12 step (iii) using the product of step (ii) and 10% Pd/C in acetic acid.

Sources & evidence

ORD record
ord-a5287060883b459f8336a74f8f1e514b
Source dataset
uspto-grants-2013_01
Patent number
US08349897B2

Reaction notes

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