HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic Acid → HCID 11576374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic Acid | HCID 243 | — |
| Reactant | Reconcile | HCID 62857 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11576374 | HCID 11576374 | 92% |
Reaction Steps
In another preparation, a 5.00 g sample of fluoxetine HCl and 1.76 g of benzoic acid were dissolved in 50 mL of acetonitrile with heating. The solution was allowed to crystallize in a large evaporating dish. The resulting solid was isolated on filter paper and dried in the air to yield 5.40 g (92%) of fluoxetine HCl:benzoic acid (1:1) cocrystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08350085B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-c26fb10a2bab4fb7a5b0198e1722aa2f |
| Source note | uspto-grants-2013_01 |