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HRID1803937

反应详情

EQUATION

反应方程式

HRID 1803937 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(N2CCNCC2)c(C)c1
HCID70544

1-(2,4-Xylyl)piperazine

C12H18N2

结构：Cc1cc(Br)ccc1C(=O)O
HCID99570

4-Bromo-2-methylbenzoic acid

C8H7BrO2

PRODUCTS

生成物

1
结构：Cc1ccc(N2CCN(C(=O)c3ccc(Br)cc3C)CC2)c(C)c1
HCID58484788

未命名化合物

收率 98.8%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 1 and using 4-bromo-2-methylbenzoic acid (5 g) and 1-(2,4-dimethylphenyl)piperazine (4.6 g), the title compound (8.9 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 1