Ethyl 4-iodobenzoate → HCID 58484622, compound

HRID 1803976Notes

Reaction equation

HRID 1803976 reaction equation
I[C:2]1[CH:12]=[CH:11][C:5]([C:6]([O:8]CC)=[O:7])=[CH:4][CH:3]=1.[CH3:13][C@H:14]1[O:18][C:17](=[O:19])[NH:16][CH2:15]1>>[CH3:13][C@H:14]1[O:18][C:17](=[O:19])[N:16]([C:2]2[CH:3]=[CH:4][C:5]([C:6]([OH:8])=[O:7])=[CH:11][CH:12]=2)[CH2:15]1

Participants

3

Reactant 2

HCID 142891Ethyl 4-iodobenzoateHCID 21794662HCID 21794662, compound

Product 1

HCID 58484622HCID 58484622, compound

Procedure

By reaction and treatment in the same manner as in Preparation Example 40 and using ethyl 4-iodobenzoate and (R)-5-methyloxazolidin-2-one, the title compound (2 g) was obtained.

Workup

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 40

Sources & evidence

ORD record
ord-2ba7553e4b83416aaa46de77666caf94
Source dataset
uspto-grants-2013_01
Patent number
US08354401B2

Reaction notes

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