Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromo-4-chlorobenzoic acid → (2-Bromo-4-chlorophenyl)[4-(3,5-dimethylpyridin-2-yl)piperazin-1-yl]methanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromo-4-chlorobenzoic acid | HCID 33126 | — |
| 반응물 | 1-(3,5-Dimethylpyridin-2-yl)piperazine | HCID 58484496 | — |
| 생성물 | (2-Bromo-4-chlorophenyl)[4-(3,5-dimethylpyridin-2-yl)piperazin-1-yl]methanone | HCID 58484730 | 98.7% |
반응 단계
By reaction and treatment in the same manner as in Preparation Example 60 and using 2-bromo-4-chlorobenzoic acid (2.09 g) and 1-(3,5-dimethylpyridin-2-yl)piperazine (1.7 g) described in Preparation Example 47, the title compound (3.58 g) was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08354401B2 |
| 출처 데이터셋 | uspto-grants-2013_01 |
| ORD ID | ord-e577c9fec5c54bf393cef204d27c4d72 |
| 출처 메모 | uspto-grants-2013_01 |