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HRID1804125

反应详情

EQUATION

反应方程式

HRID 1804125 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1ccc(Br)cc1N1CCCS1(=O)=O
HCID54933008

未命名化合物

结构：CCc1cnc(N2CCNCC2)c(C)c1
HCID58484578

未命名化合物

PRODUCTS

生成物

1
结构：CCc1cnc(N2CCN(C(=O)c3ccc(Br)cc3N3CCCS3(=O)=O)CC2)c(C)c1
HCID58484567

未命名化合物

收率 94.1%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 90 and using 4-bromo-2-(1,1-dioxoisothiazolidin-2-yl)benzoic acid (4.80 g) described in Preparation Example 178 and 1-(5-ethyl-3-methylpyridin-2-yl)piperazine (3.08 g) described in Preparation Example 53, the title compound (7.16 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 90
  3. customdescribed in Preparation Example 53