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HRID1804126

反应详情

EQUATION

反应方程式

HRID 1804126 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(N2CCNCC2)c(C)c1
HCID70544

1-(2,4-Xylyl)piperazine

C12H18N2

结构：O=C(O)c1ccc(Br)cc1N1CCCS1(=O)=O
HCID54933008

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(N2CCN(C(=O)c3ccc(Br)cc3N3CCCS3(=O)=O)CC2)c(C)c1
HCID58484743

未命名化合物

收率 101.3%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 90 and using 4-bromo-2-(1,1-dioxoisothiazolidin-2-yl)benzoic acid (661 mg) described in Preparation Example 178 and 1-(2,4-dimethylphenyl)piperazine (431 mg), the title compound (1.03 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 90