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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1804593Erstellt: 25. Oktober 2026

tert-butyl 4-(1H-pyrazol-1-yl)piperidine-1-carboxylate → 4-(1H-Pyrazol-1-yl)piperidine

https://huagongshe.com/reaction/1804593

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukttert-butyl 4-(1H-pyrazol-1-yl)piperidine-1-carboxylateHCID 67971778—
LösungsmittelHydrochloric AcidHCID 313—
Lösungsmittel1,4-DioxaneHCID 31275—
Produkt4-(1H-Pyrazol-1-yl)piperidineHCID 2119304596%

Reaktionsschritte

The title compound from Step B above (50 mg, 0.2 mmol) was dissolved in 4 M HCl in dioxane (2.0 mL) and stirred at RT for 1 h. The product was concentrated under reduced pressure and dried under high vacuum to give the title compound (i-17) (30 mg, 96%). ESI-MS calculated for C81H13N3: Exact Mass: 151.11. Found 152.10.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08354403B2
Quelldatensatzuspto-grants-2013_01
ORD IDord-82c09d36b50e44e199295577f8c352ee
Quellennotizuspto-grants-2013_01