HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl 4-(2H-tetrazol-5-YL)piperidine-1-carboxylate → HCID 178420016, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl 4-(2H-tetrazol-5-YL)piperidine-1-carboxylate | HCID 18187701 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 178420016 | HCID 178420016 | 98% |
Reaction Steps
The title compound from Step A above (197 mg, 0.77 mmol) was dissolved in 4 M HCl in dioxane (3.0 mL) and stirred at RT for 1 h. The product was concentrated under reduced pressure and dried under high vacuum to give the title compound (i-32) (116 mg, 98%). ESI-MS calculated for C6H11N5: Exact Mass: 153.13. Found 154.12.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354403B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-3c86442f04464d67a458e3769da53e97 |
| Source note | uspto-grants-2013_01 |