HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoethanol → 2-(2-tert-Butyl-5-aminophenoxy)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoethanol | HCID 10898 | — |
| Reactant | 2-Tert-butyl-5-nitrophenol | HCID 21959617 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 2-(2-tert-Butyl-5-aminophenoxy)ethanol | HCID 57470212 | — |
Reaction Steps
2-(2-tert-Butyl-5-aminophenoxy)ethanol (C-4) was synthesized following the general scheme above starting from 2-tert-butyl-5-nitrophenol (C-1-a) and 2-bromoethanol. HPLC ret. time 2.08 min, 10-99% CH3CN, 5 min run; ESI-MS 210.3 m/z (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354427B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-4887ba11728043bf9a3ca1ec3436b820 |
| Source note | uspto-grants-2013_01 |