HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-3-isothiocyanatopyridine → N-(3-Phenoxy-5-(pyridin-4-ylthio)pyridin-2-yl)thiazolo[5,4-b]pyridin-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-3-isothiocyanatopyridine | HCID 12868088 | — |
| Reactant | 3-Phenoxy-5-(pyridin-4-ylthio)pyridin-2-amine | HCID 66995453 | — |
| Product | N-(3-Phenoxy-5-(pyridin-4-ylthio)pyridin-2-yl)thiazolo[5,4-b]pyridin-2-amine | HCID 57742566 | — |
Reaction Steps
Prepared according to the method of Example 292 from 2-chloro-3-isothiocyanatopyridine (0.116 g, 0.677 mmol) and 3-phenoxy-5-(pyridin-4-ylthio)pyridin-2-amine. 1H NMR (d6-DMSO) δ 7.10 (d, 2H), 7.17-7.23 (m, 3H), 7.40-7.47 (m, 4H), 7.97 (bs, 1H), 8.36-8.41 (m, 4H), 11.88 (bs, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354540B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-0dcd73bd01b1453aaf12186097cb99ef |
| Source note | uspto-grants-2013_01 |