Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(2-Methanesulfonylethyl)(methyl)amine → HCID 16037910, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (2-Methanesulfonylethyl)(methyl)amine | HCID 3856040 | — |
| 반응물 | Sodium triacetoxyborohydride | HCID 5049666 | — |
| 반응물 | 3-[1-(ethylsulfonyl)-4-piperidinyl]-5-(3-formylphenyl)-1H-indole-7-carboxamide | HCID 57732804 | — |
| 생성물 | HCID 16037910 | HCID 16037910 | 31% |
반응 단계
Following the general procedure of example 1, 3-[1-(ethylsulfonyl)-4-piperidinyl]-5-(3-formylphenyl)-1H-indole-7-carboxamide (42.0 mg, 0.096 mmol), N-methyl-2-(methylsulfonyl)ethanamine (12.0 mg, 0.087 mmol) and NaBH(OAc)3 (58.0 mg, 0.261 mmol) were reacted to give the title compound (15.1 mg, 28.0%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08354406B2 |
| 출처 데이터셋 | uspto-grants-2013_01 |
| ORD ID | ord-7c3ee9df27704347be169b6104da478e |
| 출처 메모 | uspto-grants-2013_01 |