HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 66723272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 66722805 | HCID 66722805 | — |
| Product | HCID 66723272 | HCID 66723272 | 15.3% |
Reaction Steps
The title compound was prepared according to the general procedure of 3-[1-(ethylsulfonyl)-4-piperidinyl]-5-{4-[(methylamino)methyl]-2-thienyl}-1H-indole-7-carboxamide trifluoroacetate, substituting dimethylamine (0.5 mL) for 2 M methylamine to afford 9 mg of the title compound (15.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354406B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-9ebd9b5f4469466dbe2d2ba8edcd4ebb |
| Source note | uspto-grants-2013_01 |