HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 66723198, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 66723506 | HCID 66723506 | — |
| Product | HCID 66723198 | HCID 66723198 | 62.7% |
Reaction Steps
The title compound was prepared according to the general procedure of 3-[1-(ethylsulfonyl)-4-piperidinyl]-5-{2-fluoro-5-[(methylamino)methyl]phenyl}-1H-indole-7-carboxamide trifluoroacetate, substituting 2-methyl-1-butanamine (38 μL, 0.524 mmol) for methanamine to afford 16.2 mg of the title compound (62.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354406B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-b4e4cef2a6f94a6a89ec44933d52f9bc |
| Source note | uspto-grants-2013_01 |