HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → Potassium 4-hydroxy-2,2-dimethylbutyrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 2,2-Dimethyl-4-butyrolactone | HCID 94746 | — |
| Solvent | Water | HCID 962 | — |
| Product | Potassium 4-hydroxy-2,2-dimethylbutyrate | HCID 23712640 | 1,783.1% |
Reaction Steps
Step A A mixture of 2,2-dimethylbutyrolactone (6.84 g, 60 mmol) and KOH (3.36 mmol) in H2O (60 mL) was heated at reflux for 2 h. The solution was cooled to room temperature and concentrated to dryness to give 4-hydroxy-2,2-dimethyl-butanoic acid monopotassium salt as a white solid (10.2 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354444B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-c42223db34144dae94020c94f94a2732 |
| Source note | uspto-grants-2013_01 |