HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → HCID 11805402, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | L-Proline | HCID 145742 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 11805402 | HCID 11805402 | — |
Reaction Steps
A mixture of rac-proline (1.15 g), ethyl acrylate (1.20 g), toluene (80 ml) and paraformaldehyde (3.6 g) was heated to reflux for 3 hours. The mixture was concentrated and the residue was filtered through silica gel. The product with the molecular weight of 183.25 (C10H17NO2); MS (ESI): 184 (M+H+) was obtained in this way.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08357686B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-8523ae32f4bb449ba5018e0fbc4fc274 |
| Source note | uspto-grants-2013_01 |