HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indazolinone → 3-Oxo-3H-indazole-1,2-dicarboxylic acid bis(2-methylbenzylamide)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indazolinone | HCID 81829 | — |
| Reactant | 1-(Isocyanatomethyl)-2-methylbenzene | HCID 2733386 | — |
| Product | 3-Oxo-3H-indazole-1,2-dicarboxylic acid bis(2-methylbenzylamide) | HCID 68458388 | — |
Reaction Steps
In analogy to example 11, 300 mg (2.24 mmol) of 1H-indazol-3-ol were reacted with 395.5 mg (2.69 mmol) of 1-isocyanatomethyl-2-methylbenzene. Yield: 177 mg (18%), M+H+: 429.26.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08357698B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-af8b008f0d1344f7a4647d52375d763f |
| Source note | uspto-grants-2013_01 |