HRID1808651

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：[Cu].c1ccc2c(c1)C1=NC2=NC2=NC(=NC3=NC(=NC4=NC(=N1)c1ccccc14)c1ccccc13)c1ccccc12

HCID475701

未命名化合物

PRODUCTS

生成物

结构：[Cu].c1ccc2c(c1)-c1nc-2nc2[n-]c(nc3nc(nc4[n-]c(n1)c1ccccc41)-c1ccccc1-3)c1ccccc21

HCID499989

[29H,31H-Phthalocyaninato(2-)-kappaN29,kappaN31]cuprate(2-)

C32H16CuN8-2

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8117

Diethylene glycol

C4H10O3

PROCEDURE

实验过程

An aliquot (400 parts) of the α-copper phthalocyanine pigment (C-2) obtained in Production Example 11(2) and containing copper monomethylphthalocyanine, common salt (1,600 parts) and diethylene glycol (400 parts) were milled for 6 hours in a kneader while controlling the temperature of the contents at 80 to 100° C. The resulting contents were subjected to treatment with a dilute acid and then to filtration. The thus-collected solids were washed with water, and then dried to obtain a fine β-copper phthalocyanine pigment (C-4) containing copper monomethylphthalocyanine.

WORKUP

后处理

customwere milled for 6 hours in a kneader
customat 80 to 100° C
filtrationto filtration
washThe thus-collected solids were washed with water
customdried

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-ed0274317de9416ea5b0fea27ebeb537
来源数据集: uspto-grants-2013_01
DOI: 10.6084/m9.figshare.5104873.v1
专利: US08361218B2
来源说明: uspto-grants-2013_01

反应 SMILES

[CH:1]1[CH:6]=[C:5]2[C:7]3[N:22]=[C:21]([C:4]2=[CH:3][CH:2]=1)[N:20]=[C:19]1[C:23]2[C:28]([C:17](=[N:18]1)[N:16]=[C:15]1[C:29]4[C:34]([C:13](=[N:14]1)[N:12]=[C:11]1[C:35]5[C:40]([C:9](=[N:10]1)[N:8]=3)=[CH:39][CH:38]=[CH:37][CH:36]=5)=[CH:33][CH:32]=[CH:31][CH:30]=4)=[CH:27][CH:26]=[CH:25][CH:24]=2.[Cu:41]>C(O)COCCO>[CH:25]1[CH:24]=[C:23]2[C:19]3[N-:18][C:17]([C:28]2=[CH:27][CH:26]=1)=[N:16][C:15]1=[N:14][C:13]([C:34]2[C:29]1=[CH:30][CH:31]=[CH:32][CH:33]=2)=[N:12][C:11]1[N-:10][C:9](=[C:40]2[C:35]=1[CH:36]=[CH:37][CH:38]=[CH:39]2)[N:8]=[C:7]1[C:5]2[C:4]([C:21](=[N:22]1)[N:20]=3)=[CH:3][CH:2]=[CH:1][CH:6]=2.[Cu:41]