HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxybenzaldehyde → 4-(3-Chloropropoxy)-M-anisaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxybenzaldehyde | HCID 101 | — |
| Reactant | Vanillin | HCID 1183 | — |
| Reactant | Salicylaldehyde | HCID 6998 | — |
| Reactant | 1-Bromo-2-Chloroethane | HCID 7849 | — |
| Reactant | Isovanillin | HCID 12127 | — |
| Product | 4-(3-Chloropropoxy)-M-anisaldehyde | HCID 4610841 | — |
| Product | HCID 12793356 | HCID 12793356 | — |
| Product | HCID 17620908 | HCID 17620908 | — |
| Product | 3-(3-Chloropropoxy)-4-methoxybenzaldehyde | HCID 23143898 | — |
Reaction Steps
2-(3-chloropropoxy)benzaldehyde, 3-(3-chloropropoxy)-4-methoxybenzaldehyde and 4-(3-chloropropoxy)-3-methoxybenzaldehyde were prepared using corresponding aldehydes such as salicylaldehyde, isovanillin and vanillin. 3-(2-chloroethoxy)-benzaldehyde was prepared by treating 3-hydroxybenzaldehyde with 1-bromo-2-chloroethane using the similar method described above.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08361996B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-efb2bfa5c2c9405bac6ec90fa1e1f73e |
| Source note | uspto-grants-2013_01 |