HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dichloropyridine → HCID 67094894, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dichloropyridine | HCID 16988 | — |
| Reactant | Pyridine, 2,3,5-trichloro- | HCID 27666 | — |
| Reactant | HCID 67094559 | HCID 67094559 | — |
| Product | HCID 67094894 | HCID 67094894 | 89% |
Reaction Steps
The procedure of Example 6 was repeated except for using 8-(6-(trifloromethyl)-1H-benzo[d]imidazol-2-yl)-3,4-dihydro-2H-benzo[b][1,4]oxazine and 2,3,5-trichloropyridine instead of 4-(5-tert-butyl-1H-benzo[d]imidazol-2-yl)benzenamine and 2,3-dichloropyridine in Example 6 respectively to obtain the title compound (4.1 g, yield: 89%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08362012B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-966ffca23db9426c8ca9cc87442b9968 |
| Source note | uspto-grants-2013_01 |