Acetylacetone → [2-(3,5-Dimethyl-pyrazol-1-yl)-9-methyl-9H-purin-6-yl]-(4-nitro-phenyl)-amine

HRID 1809262Notes

Reaction equation

HRID 1809262 reaction equation
[NH:1]([C:3]1[N:11]=[C:10]2[C:6]([N:7]=[CH:8][N:9]2[CH3:12])=[C:5]([NH:13][C:14]2[CH:19]=[CH:18][C:17]([N+:20]([O-:22])=[O:21])=[CH:16][CH:15]=2)[N:4]=1)[NH2:2].[CH3:23][C:24](=O)[CH2:25][C:26](=O)[CH3:27]>>[CH3:23][C:24]1[CH:25]=[C:26]([CH3:27])[N:1]([C:3]2[N:11]=[C:10]3[C:6]([N:7]=[CH:8][N:9]3[CH3:12])=[C:5]([NH:13][C:14]3[CH:15]=[CH:16][C:17]([N+:20]([O-:22])=[O:21])=[CH:18][CH:19]=3)[N:4]=2)[N:2]=1

Participants

3

Procedure

Was prepared according to Example 9 from (2-hydrazino-9-methyl-9H-purin-6-yl)-(4-nitro-phenyl)-amine and 2,4-pentanedione.

Workup

  1. customWas prepared

Sources & evidence

ORD record
ord-8f10085ee56c4299a2e456a969e117ef
Source dataset
uspto-grants-2013_01
Patent number
US08362024B2

Reaction notes

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