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HRID1809524

反应详情

EQUATION

反应方程式

HRID 1809524 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)c1cc(Br)cc(OC(F)(F)F)c1
HCID53419621

未命名化合物

结构：COC(=O)c1cc(C#N)cc(OC(C)C)c1
HCID67195394

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1cc(C#N)cc(OC(F)(F)F)c1
HCID67192787

Benzoic acid, 3-cyano-5-(trifluoromethoxy)-, methyl ester

C10H6F3NO3

PROCEDURE

实验过程

Prepared from methyl 3-bromo-5-(trifluoromethoxy)benzoate according to the procedure for methyl 3-cyano-5-isopropoxybenzoate. LCMS-ESI (m/z) calculated for C10H6F3NO3: 245.2; no m/z observed, tR=4.43 min. 1H NMR (400 MHz, CDCl3) δ 8.27 (t, J=1.4 Hz, 1H), 8.16-8.07 (m, 1H), 7.73-7.65 (m, 1H), 3.99 (s, 3H).