HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluidine → HCID 86761761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluidine | HCID 7813 | — |
| Reactant | Butanoic acid, 4-chloro-3-oxo- | HCID 119720 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | Hydrate;hydrochloride | HCID 21885828 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Product | HCID 86761761 | HCID 86761761 | — |
Reaction Steps
4-Methyl aniline (4 g, 37.38 mmol) was suspended in water: HCl (2:1); 30 ml. Aqueous solution of sodium nitrite (2.57 g, 37.38 mmol) was added at 0°-5° C. over a period of 30 minutes. Subsequently, aqueous solution of chloroacetoacetic acid (6.63 g, 48.59 mmol) was added followed by aqueous solution of sodium acetate (6.13 g, 74.76 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08362064B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-7cb8b72efa6b4331a1f2cb95b0d0c0e3 |
| Source note | uspto-grants-2013_01 |