HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 3-bromo-4-methoxyphenylacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 3-Bromo-4-methoxyphenylacetic acid | HCID 136615 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | Ethyl 3-bromo-4-methoxyphenylacetate | HCID 57419861 | — |
Reaction Steps
A solution of 3-bromo-4-methoxyphenylacetic acid (3.0 g, 12.2 mmol) in EtOH and sulfuric acid was stirred at 100° C. for 2 hours. The mixture was concentrated and partitioned between EtOAc and H2O, and the organic layer was separated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08362044B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-0762c72c8f7a4578835a3b02e9b9ed23 |
| Source note | uspto-grants-2013_01 |