2-Aminophenol → HCID 22501646, compound

HRID 1813877Notes

Reaction equation

HRID 1813877 reaction equation
[OH:1][C:2]1[CH:8]=[CH:7][CH:6]=[CH:5][C:3]=1[NH2:4].[N:9]([C:12]1[CH:17]=[CH:16][C:15]([CH2:18][C:19]([O:21]C)=[O:20])=[CH:14][CH:13]=1)=[C:10]=[O:11]>>[OH:1][C:2]1[CH:8]=[CH:7][CH:6]=[CH:5][C:3]=1[NH:4][C:10](=[O:11])[NH:9][C:12]1[CH:13]=[CH:14][C:15]([CH2:18][C:19]([OH:21])=[O:20])=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 58012-AminophenolHCID 11183116HCID 11183116, compound

Product 1

HCID 22501646HCID 22501646, compound

Procedure

4-(2-Hydroxyphenylureido)phenylacetic acid was prepared using procedure C with 2-hydroxyaniline and KCl: 1H NMR (CD3SOCD3, 300 MHz, ppm) 9.90 (s, 1H), 9.25 (s, 1H), 8.12 (s, 1H), 8.02 (bd, 1H), 7.37 (d, 2H), 7.13 (d, 2H), 6.70-6.97 (m, 3H), 3.48 (s, 2H).

Sources & evidence

ORD record
ord-2f29408414104ae4bf63900d8ec89679
Source dataset
uspto-grants-2005_04
Patent number
US06875743B1

Reaction notes

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