Cyclohexanone → Cyclohexylidene(2-thienyl)acetonitrile

HRID 1814044Notes

Reaction equation

[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH2:6][C:7]#[N:8].[C:9]1(=O)[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1>>[C:9]1(=[C:6]([C:2]2[S:1][CH:5]=[CH:4][CH:3]=2)[C:7]#[N:8])[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1

Participants

Reactant 2

HCID 7967Cyclohexanone

HCID 728802-Thienylacetonitrile

Product 1

HCID 22505734Cyclohexylidene(2-thienyl)acetonitrile

Procedure

The expected intermediate is obtained in the manner described in General Protocol A starting from 2-thienylacetonitrile and cyclohexanone.

Sources & evidence

ORD record: ord-a1c3b5e830e4482c8d4d5686149aefc5
Source dataset: uspto-grants-2005_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06875788B2

Reaction notes

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